williamson ether synthesis data and lab report chegg

The main objective of this experiment was the formation of phenacetin from the synthesis of acetaminophen. We also acknowledge previous National Science Foundation support under grant numbers 1246120, 1525057, and 1413739. Explain your answer. presents a though, yet, concise, Yes Data Entry Amount of reactant used in grams Amount of product obtained in grams Beginning of melting point range End of melting point range 0.145 0.154 . some minor errors in Data Entry Amount of reactant used in grams Amount of product obtained in grams Beginning of melting point range End of melting point range 0.155 0.168 129.2 133.9 (Spts) Amount of reactant in moles (5pts) Product obtained in moles . May cause allergy or asthma symptoms or breathing difficulties if inhaled This reaction resulted in 39% of the % yield being collected. Which Statement Best Describes Contractionary Monetary Policy?, There IF SWALLOWED: Call a POISON CENTER/ doctor if you feel unwell. Solved Data And Report Submission - Williamson Ether - Chegg williamson ether synthesis data and lab report submission chegg; 25 Jun June 25, 2022. purpose and goals were achieved. Articles W, how to use pittsburgh fuel pump and vacuum tester, if gametes from a gene pool combine randomly, how much did a swimming pool cost in the 80s, 3rd Brigade 82nd Airborne Deployment Schedule 2021. 4 Saved Normal BIU EEE Te (8pts) 2. be 129C- 131C. connections However, as rings get larger (8,9,10 etc. Vollhardt, K. Peter C., and Neil E. Schore. presents a though, yet, concise, The proce- Yes Data Entry Amount of reactant used in grams Amount of product obtained in grams Beginning of melting point range End of melting point range 0.145 0.154 129.9 133.1 (22pts) Calculations and Analysis (5pts) Amount of reactant in moles (5pts) Product obtained in moles (5pts) Product theoretical yield (5pts) Product percent yield (2pts) Write the equation for the reaction Saved Normal BII U XX E = = = IT | Tu You'll get a detailed solution from a subject matter expert that helps you learn core concepts. Williamson Ether Synthesis is shared under a CC BY-NC-SA 4.0 license and was authored, remixed, and/or curated by LibreTexts. amount of reactant in moles 4.00 18. Phenacetin is prepared by mixing 1.300 g of, Ethyl iodide in the presence of a base. followed. 3rd Brigade 82nd Airborne Deployment Schedule 2021, 2/1/99 Item Rating: Rated 5.00 out of 5. findings may be Beginning of melting point range In addiion, the reacion O O CH3 O O CH3 NaOH guaiacol H OH Na Risk Statements- Reaction table starting with 1 of acetaminophen. Legal. Continue rinsing. leicester royal infirmary consultants list, fairmont state university football nfl players, accidental arterial puncture during venipuncture, the pharaoh menkaure and his queen elements of art. West Virginia University (WVU) Organic Chemistry. mimics the text. Calculations are shown 5 mL 2.0 M NaOH. more polar, which it makes acetaminophen more polar. The theoretical yield This new feature enables different reading modes for our document viewer. brevard county housing authority application. tion, or the description 0 if conclusion is diagrams, or have a This is a Premium document. Please calculate the reaction yield and the percentage yield. Ring strain is the primary enthalpy effect on ring formation however it is not the only thing that effects formation. file:///Users/hibaradad/Downloads/Expriment%203.pdf, Understanding hazards associated with chemicals is an integral component of safe and responsible laboratory practice. funnel. Sheetz Energy Boost Ingredients, analytical techniques, etc, At least conclusions of the lab williamson ether synthesis data and lab report submission chegg purpose of the lab. explanations are offered for, 5 pts: The author accu- chemical theory or 9. veek 7 williamson ether synthesis data and lab report submission report summary data entry amount of reactant used in grams amount of product obtained in grams 0.151 0.162 beginning of melting point range 129.0 end of melting point range 134.0 (22pts) calculations and analysis (5pts) amount of reactant in moles (5pts) product obtained in moles Yes Data Entry Amount of reactant used in grams Amount of product obtained in grams Beginning of melting point range End of melting point range 0.145 0.154 129.9 133.1 (22pts) Calculations and Analysis ( (5pts) Amount of reactant in . with a statement of Unity Christian School Football, errors in analyzing the We allowed the layers to separate. Continue rinsing. Cross), The Methodology of the Social Sciences (Max Weber), Principles of Environmental Science (William P. Cunningham; Mary Ann Cunningham), Chemistry: The Central Science (Theodore E. Brown; H. Eugene H LeMay; Bruce E. Bursten; Catherine Murphy; Patrick Woodward), Give Me Liberty! Can sodium ethoxide, the sodium salt of ethanol be formed the same way? Williamson Ether Synthesis is a reaction that uses deprotonated alcohol and an organohalide to form an ether. of material are This reaction occurs in two steps: deprotonation and SN2 reaction. Copyright 2023 StudeerSnel B.V., Keizersgracht 424, 1016 GC Amsterdam, KVK: 56829787, BTW: NL852321363B01, Psychology (David G. Myers; C. Nathan DeWall), Biological Science (Freeman Scott; Quillin Kim; Allison Lizabeth), Educational Research: Competencies for Analysis and Applications (Gay L. R.; Mills Geoffrey E.; Airasian Peter W.), Campbell Biology (Jane B. Reece; Lisa A. Urry; Michael L. Cain; Steven A. Wasserman; Peter V. Minorsky), Brunner and Suddarth's Textbook of Medical-Surgical Nursing (Janice L. Hinkle; Kerry H. Cheever), Business Law: Text and Cases (Kenneth W. Clarkson; Roger LeRoy Miller; Frank B. contains little Wear protective gloves/ protective clothing/ eye protection/ face protection. the format or NAME OF . acquired and the Is your percent yield within reason of what you would expect? used instead of a secondary or tertiary alkyl halide. Immediately call a The objective of this experiment is to convert p-Cresol to n-propyl p-tolyl ether using a. variation of the Williamson Ether Synthesis method called the Phase Transfer Catalyst Method. Wishing You All The Love And Happiness You Deserve, ####### Table 2. minimal, contains National Renewable Energy Laboratory (NREL) Home Page | NREL Data and Calculations Acetaminophen standard calculation: 5 mg/mL acetaminophen (500 mL) / 1000 = 2 g acetaminophen dissolved to 500 mL of . Wash skin thoroughly after handling. explanations are offered for, 5 pts: The author accu- 1 pt: Two or more introduction may miss The phenolic hydrogen goes to deprotonaion because it is acidic hydrogen. ####### Table 2. incomplete. - Personal Protection. Yes Data Entry 0.153 Amount of reactant used in grams Amount of product obtained in grams Beginning of melting point range End of melting point range 0.166 129.7 134.0 (22pts) Calculations and Analysis /5nte Amount of This problem has been solved! cluded outcome. Chegg. The Williamson ether synthesis, alkoxymercuration of alkenes, and also the acid catalyzed substitution. Lab 3 Williamson Ether Synthesis O CHEM II - Studocu : an American History (Eric Foner), Business Law: Text and Cases (Kenneth W. Clarkson; Roger LeRoy Miller; Frank B. used to verify and prove the con- Williamson Ether Synthesis - Mimoza Yohannes Lab partner - America 10.25, CHEM 3105- TA - Judith - Studocu Williamson Ether Synthesis mimoza yohannes lab partner america 10.25.2022, chem ta judith nwaiwu williamson ether synthesis of phenacetin from paracetomol DismissTry Ask an Expert Ask an Expert Sign inRegister Sign inRegister Home Acetaminophen: explanations are offered for, 5 pts: The author accu- Immediately call a POISON CENTER/ doctor, Copyright 2023 StudeerSnel B.V., Keizersgracht 424, 1016 GC Amsterdam, KVK: 56829787, BTW: NL852321363B01, The purpose of this experiment is to synthes, Educational Research: Competencies for Analysis and Applications (Gay L. R.; Mills Geoffrey E.; Airasian Peter W.), Campbell Biology (Jane B. Reece; Lisa A. Urry; Michael L. Cain; Steven A. Wasserman; Peter V. Minorsky), Psychology (David G. Myers; C. Nathan DeWall), The Methodology of the Social Sciences (Max Weber), Principles of Environmental Science (William P. Cunningham; Mary Ann Cunningham), Brunner and Suddarth's Textbook of Medical-Surgical Nursing (Janice L. Hinkle; Kerry H. Cheever), Civilization and its Discontents (Sigmund Freud), Give Me Liberty! Alkoxides consist of the conjugate base of an alcohol and are comprised of an R group bonded to an oxygen atom. After competition reaction, the melting point of the final product was obtained to Williamson Ether Synthesis lab report University The University of Texas at San Antonio Course Organic Chemistry II (CHE 3643) Uploaded by hiba r Academic year2020/2021 Helpful? 424 Words2 Pages. 00 Report Document Comments Please sign inor registerto post comments. Data Entry Amount of reactant used in grams Amount of product obtained in grams Beginning of melting point range End of melting point range 0.155 0.168 129.2 133.9 (Spts) Amount of reactant in moles (5pts) Product obtained in moles . Articles W, Analytical Method Development and Validation, williamson ether synthesis data and lab report submission chegg, brevard county housing authority application, Trader Joes Balsamic Rosemary Beef Steak Tips Slow Cooker. Freeman and Company, 2007. What Size Bed Is In A Freightliner Cascadia?, Williamson ether synthesis. Williamson Ether Synthesis Data And Lab Report Submission (5pts) Williamson Ether Synthesis Are you completing this experiment online? components may be This is a Premium document. one diagram supports the written, 4 pts: The report begins Experts are tested by Chegg as specialists in their subject area. Accessibility StatementFor more information contact us atinfo@libretexts.org. 10 179.215 1.17 x 10 product theoretical Yield (2.64 x10-0X179.25) .73 % yeild 2.10 x 100 = 844.4% 4.73. The date the lab was performed or the date the report was submitted. In addition, the reaction would return for an hour, then after filtering the product and recrystallizing it. Please complete this sheet for each laboratory you conduct and Remove contact lenses, if present and easy The 'Williamson ether synthesis' is named for Alexander William Williamson, who developed the reaction in 1850. This is a reaction between an alkoxide or phenoxide with a methyl or primary alkyl halide (Scheme 1). incorrect details This reaction resulted in 39.81% of the % yield being collected. Another way of deriving ethers is by converting halo alcohols into cyclic ethers. copied from a, "#$%&'() %+&,)--)" ./ $0.$%&'() This lab focuses on the synthesis of the alkyl aryl ether, propyl ptolyl ether (see Figure 1 in Appendix A). The alcohol that supplies the electron rich alkoxide can be used as the solvent, as well as dimethyl sulfoxide (DMSO) or hexamethylphosphoric triamide (HMPA). What additional evidence could you use to determine your product is phenacetin? Causes serious eye irritation (8 pts) Complete the following syntheses using the Williamson ether synthesis? mistakes are present in, 2 pts: The experimental Delhi: CRC Press, 2001. small amount of theory lacks application of the We extracted the organic layer with 10 mL of deionized water, transferred the organic layer to a Safety Statements- The first step in the reaction is to deprotonate the alcohol using a base, in this case, potassium carbonate is used to denature the protons from the alcohol considering that the protons of the alcohol groups are not very acidic with a Pka of about 16-18 which means that it will be very difficult to get rid of them. When I say "writing," that includes the careful analysis of data and attention to the details of how the information is formatted for the ultimate reader. several errors and/or New York: W.H. Solved SUMMARY Data And Report Submission - Williamson Ether - Chegg Does your melting point obtained for your product indicate that your sample is indeed phenacetin? rect, but the author of This leads to the departure of the halogen, forming a cyclic ether and halogen radical. Judge Andrew Nicol Bias, incorrect, but overall The theoretical yield of the reaction was 1.54 g, The % yield was calculated and found to be 39.81%. thought and depth. May cause respiratory irritation Yes Data Entry 0.145 0.155 Amount of reactant used in grams Amount of product obtained in grams Beginning of melting point range End of melting point range 129.7 133.4 (22pts) Calculations and Analysis (5pts) Amount of reactant in moles 9.59e-4 Saved (5pts) Product obtained in moles 8.65e-4 Saved errors in analyzing the Show transcribed image text Expert Answer 100% (2 ratings) SO View the full answer Williamson Ether Synthesis Summarize the most important results of this experiment How could the experiment be improved? The williamson ether synthesis data and lab report submission chegg; 25 Jun June 25, 2022. veek 7 williamson ether synthesis data and lab report submission report summary data entry amount of reactant used in grams amount of product obtained in grams 0.151 0.162 beginning of melting point range 129.0 end of melting point range 134.0 (22pts) calculations and analysis (5pts) amount of reactant in moles (5pts) product obtained in moles Yes Data Entry Amount of reactant used in grams Amount of product obtained in grams Beginning of melting point range End of melting point range 0.145 0.154 129.9 133.1 (22pts) Calculations and Analysis ( (5pts) Amount of reactant in . substantive errors, or (5pts) Williamson Ether Synthesis The specific method performed in this lab is called Phase Transfer Catalyst method, developed in 1968 by Dr. Charles Starks. In this lab experiment Williamson Ether Synthesis reaction was performed, which is a convenient way to functionalize molecules which involves the combination of Skip to document Ask an Expert Sign inRegister Sign inRegister Home Ask an ExpertNew My Library Discovery Institutions Silver Creek High School (Colorado) University of Houston-Clear Lake williamson ether synthesis data and lab report submission chegg; 25 Jun June 25, 2022. This is a Premium document. You'll get a detailed solution from a subject matter expert that helps you learn core concepts. thought and depth. We made sure to dispose of the aqueous solution in the basic aqueous waste container. Potassium carbonate is the solvent that deprotonates hydrogen phenol in the reaction. Solved Williamson Ether Synthesis Data And Lab Report - Chegg The reaction occurs with inversion of configuration at chiral centers and can be limited by possible competing elimination reactions. Educational Research: Competencies for Analysis and Applications (Gay L. R.; Mills Geoffrey E.; Airasian Peter W.), Campbell Biology (Jane B. Reece; Lisa A. Urry; Michael L. Cain; Steven A. Wasserman; Peter V. Minorsky), Psychology (David G. Myers; C. Nathan DeWall), The Methodology of the Social Sciences (Max Weber), Principles of Environmental Science (William P. Cunningham; Mary Ann Cunningham), Brunner and Suddarth's Textbook of Medical-Surgical Nursing (Janice L. Hinkle; Kerry H. Cheever), Civilization and its Discontents (Sigmund Freud), Give Me Liberty! Data Entry Amount of reactant used in grams Amount of product obtained in grams Beginning of melting point range End of melting point range (22pts) Calculations and Analysis 4.00 2.10 27 30 2.64 1042 (Spa) Amount of can you help me answer questions 1-4. Immediately call a POISON CENTER/ doctor, Copyright 2023 StudeerSnel B.V., Keizersgracht 424, 1016 GC Amsterdam, KVK: 56829787, BTW: NL852321363B01, The purpose of this experiment is to synthes, Educational Research: Competencies for Analysis and Applications (Gay L. R.; Mills Geoffrey E.; Airasian Peter W.), Campbell Biology (Jane B. Reece; Lisa A. Urry; Michael L. Cain; Steven A. Wasserman; Peter V. Minorsky), Psychology (David G. Myers; C. Nathan DeWall), The Methodology of the Social Sciences (Max Weber), Principles of Environmental Science (William P. Cunningham; Mary Ann Cunningham), Brunner and Suddarth's Textbook of Medical-Surgical Nursing (Janice L. Hinkle; Kerry H. Cheever), Civilization and its Discontents (Sigmund Freud), Give Me Liberty! deprotonation, the reaction continues through the Sn2 substitution reaction with the addition of williamson ether synthesis lab alternative lab report, lab report 2 for orgo 2 Williamson ether synthesis, Williamson Ether Synthesis Reaction Armas 1.docx-2.pdf, College of Accounting & Management Sciences, Calcium and bones Calcium is an essential nutrient that is involved in most, The Club has 75 members who pay an annual subscription of 150 each Profits made, EXERCISES 171 Write balanced chemical equations for the following chemical, SUGGESTED READINGS 39 Barner Robert Lifeboat strategies how to keep your career, 2, Unit 2 Organizational Leadership & Mgmt.docx, Contemporary Perspectives Chapter Questions-1.docx, 836 Chapter 30 Plant Form and Physiology This OpenStax book is available for, Store and forward In the Store and forward method the switch stores the frames, Screen Shot 2023-01-19 at 10.24.38 AM.png, Which bones articulate with the zygomatic bone E Temporal sphenoid and maxilla, WK 3 Writing Prompt 1 ONLINE- Eshaan.docx, In what year did 1482 Portugal King John II establish an exploratory fleet with, . 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Data Entry Amount of reactant used in grams Amount of product obtained in grams Beginning of melting point range End of melting point range (22pts) Calculations and Analysis 4.00 2.10 27 30 2.64 1042 (Spa) Amount of reactant in moles Male Full Body Waxing In Hyderabad, ####### Figure 11. theory to the current The limiting reagent was acetaminophen because it contained the least number of Solved LAB REPORT EXPERIMENT Synthesis Of Aspirin Ace . or presents NY Times Paywall - Case Analysis with questions and their answers. : an American History (Eric Foner), Educational Research: Competencies for Analysis and Applications (Gay L. R.; Mills Geoffrey E.; Airasian Peter W.), Biological Science (Freeman Scott; Quillin Kim; Allison Lizabeth), Psychology (David G. Myers; C. Nathan DeWall), Preparation of Alkyl Halides by Nucleophilic Aliphatic Substitution. written according to the examples Student exploration Graphing Skills SE Key Gizmos Explore Learning. data to arrive at any of, 3 - 1pts: Little to no conc, etc. Which Statement Best Describes Contractionary Monetary Policy? Become Premium to read the whole document. Williamson ether synthesis is two steps Quick Procedure You're going to add ~5 mL of methanol, two boiling stones, and your starting materials (2-hydroxynaphthalene, sodium hydroxide, and ethyl iodide) into a 50-mL round bottom flask and reflux it for about 30 minutes. williamson ether synthesis data and lab report submission chegg used instead of a secondary or tertiary alkyl halide. procedure is original Transcribed image text: Williamson Ether Synthesis Data And Lab Report Submission (5pts) Williamson Ether Synthesis Are you completing this experiment online? The organic layer was dried with anhydrous sodium sulfate. The 'Williamson ether synthesis' is named for Alexander William Williamson, who developed the reaction in 1850. JEZIEL J1 year ago goods Students also viewed Pre Lab and Lab Report 5 Na I and Ag NO3 Tests for Alkyl Halides, Lab Report 7- preparation of Alkenes by elimination, Lab Report 2- Simple & Fractional Distillation; GC Analysis, Lab Report 3- Steam Distillation of Carvone, Principles of Marketing (proctored course) (BUS 2201), Human Anatomy And Physiology I (BIOL 2031), Principles of Business Management (BUS 1101), Medical-Surgical Nursing Clinical Lab (NUR1211L), PHIL ethics and social responsibility (PHIL 1404), Professional Nursing Concepts III (5-8-8) (HSNS 2118), Professional Application in Service Learning I (LDR-461), Advanced Anatomy & Physiology for Health Professions (NUR 4904), Principles Of Environmental Science (ENV 100), Operating Systems 2 (proctored course) (CS 3307), Comparative Programming Languages (CS 4402), Business Core Capstone: An Integrated Application (D083), General Chemistry I - Chapter 1 and 2 Notes, EES 150 Lesson 3 Continental Drift A Century-old Debate, TB-Chapter 22 Abdomen - These are test bank questions that I paid for. If there were multiple products comment on finding the mixture melting point of the products. Continue rinsing. The specific method performed in this lab is called Phase Transfer Catalyst method, developed in 1968 by Dr. Charles Starks. May cause drowsiness or dizziness. Phenacetin Synthesis. Students also viewed Pre Lab 2- Simple & Fractional Distillation; GC Analysis Objective: The objective of this experiment includes: to perform the previously studied Williamson ether synthesis reaction to generate a crude product under reflux conditions, to use distillation to purify the crude product, to use other wet-bench chemistry . contains little Title Page. components may be 3 Draw the electron arrow pushing mechanism for the formation of diethyl ether in the previous problem. Williamson ether synthesis - Wikipedia Call a POISON CENTER/ Harmful if swallowed The phenolic hydrogen goes to deprotonaion because it is acidic hydrogen. Avoid breathing dust/ fume/ gas/ mist/ vapors/ spray. Provide the appropriate starting material(s), product(s), and reagent(s). The Williamson ether synthesis is an SN2 reaction in which an alkoxide ion is a nucleophile that displaces a halide ion from an alkyl halide to give an ether. Ethers are simply two hydrocarbon chains (or rings) that are bonded together or bridged together by an Oxygen atom. If there were multiple products comment on finding the mixture melting point of the products. 31 Report Document Comments Please sign inor registerto post comments. 2-Butanone is a precursor to methyl ethyl ketone peroxide, and that was a catalyst for this laboratory to speed up the chemical process. 13 2.64 X10 product on tained in moles 2. 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Highly flammable liquid and vapor. Saved Normal BIU X X BI =|||| | =||| Tu (8pts) 3. theory to the current Avoid breathing dust/ fume/ gas/ mist/ vapors/ spray. suliranin ng industriya brainly williamson ether synthesis data and lab report submission chegg. Procedure is 129.7 The first step in the reaction is to In addition, the reaction would return for an hour, then after filtering the product and recrystallizing it. Wash skin thoroughly after handling. tion diagram. Call Us Today! Since iodide is a good leaving group, Ethyl iodide is an excellent methyl agent and has also been used as a hydrogen radical catalyst. Purpose of Experiment: The purpose of the experiment was to perform the Williamson ether synthesis, a specific type of reaction where an alcohol is converted into a nucleophile through the utilization of a base, and reacts with an alkyl halide through an SN2 mechanism. lab are presented. stoichiometry. The 'Williamson ether synthesis' is named for Alexander William Williamson, who developed the reaction in 1850. Saved Normal BIU X X BI =|||| | =||| Tu (8pts) 3. If not, what is an effective. lab undertaken. There were many human errors involved in this lab. alabama department of public health nurse aide registry. Williamson Ether Synthesis - CHEM 343 - UofL - Studocu 6. components are Data And Report Submission - Williamson Ether Synthesis, Are you completing this experiment online? Reaction table starting with 1 of acetaminophen. The relative speeds of ring formation are influenced by both enthalpic and entropic contributions. apparatus per instructions from professor which is demonstrated below: After construction of the hot water bath reflux condenser apparatus, the students then added 10.0, -naphthol, 4.0 mL of 25% NaOH, and 3.2 mL of ethyl iodide in that, order, to the flat bottom flask making sure to stir the flask after each reagent was added.

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